| Date | Location | Result | |
| 04/21/21 | St. Augustine, Fla. | Flagler 3, UNC Pembroke 0 (25-20,25-22,25-22) | Box score |
| 04/17/21 | Young Harris, Ga. | UNC Pembroke 3, Young Harris 0 (25-11,25-13,25-11) | Box score |
| 04/16/21 | Greenwood, S.C. | Lander 3, UNC Pembroke 2 (20-25,25-18,16-25,25-18,15-10) | Box score |
| 04/09/21 | Pembroke, N.C. | Flagler 3, UNC Pembroke 1 (25-15,22-25,25-17,25-21) | Box score |
| 04/06/21 | Florence, S.C. | UNC Pembroke 3, Francis Marion 0 (25-22,25-16,26-24) | Box score |
| 04/02/21 | Augusta, Ga. | Augusta 3, UNC Pembroke 0 (25-15,25-23,25-16) | Box score |
| 03/31/21 | Aiken, S.C. | USC Aiken 3, UNC Pembroke 0 (25-22,25-22,25-20) | Box score |
| 03/26/21 | Pembroke, N.C. | UNC Pembroke 3, Young Harris 0 (25-12,25-19,25-10) | Box score |
| 03/25/21 | Pembroke, N.C. | UNC Pembroke 3, Lander 0 (25-17,25-13,25-19) | Box score |
| 03/20/21 | St. Augustine, Fla. | Flagler 3, UNC Pembroke 0 (25-12,25-19,25-11) | Box score |
| 03/19/21 | Milledgeville, Ga. | Georgia College 3, UNC Pembroke 2 (23-25,27-29,25-17,25-19,15-10) | Box score |
| 03/16/21 | Pembroke, N.C. | UNC Pembroke 3, Francis Marion 1 (24-26,25-18,25-20,25-16) | Box score |
| 03/13/21 | Pembroke, N.C. | UNC Pembroke 3, Augusta 1 (16-25,25-21,25-23,25-23) | Box score |
| 03/12/21 | Pembroke, N.C. | USC Aiken 3, UNC Pembroke 1 (21-25,25-21,25-20,25-13) | Box score |
| 03/08/21 | Pembroke, N.C. | UNC Pembroke 3, Georgia College 1 (25-11,25-16,20-25,25-23) | Box score |